MS Report from Instrument: LCMS-02 File ..18-1 2017-08-18 09-37-12\\BIZ2017-818-WYQ4.D Tgt Mass (CHM): Injection Date : 18 Aug 17 10:42 am +0800 Seq. Line : 15 Sample Name : BIZ2017-818-WYQ4 Location : P2-C-06 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\chem32\\1\\DATA\\20170818\\20170818-1 2017-08-18 09-37-12\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\DATA\\20170818\\20170818-1 2017-08-18 09-37-12\\1-POS-3MIN.M Catalog No : HY-101924 Batch#25944 A-AP-189 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 B, Sig=214,4 Ref=off mAU100075050025000.5 DAD1 C, Sig=254,4 Ref=off mAU100075050025000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7060000040000020000000.51 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.7 0.050-0.05-0.10.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min1.522.5min1.512.0511.2001.3231.522.0512.5min.968 1Area: 6.7451222.0792.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.20 0.01 1.46 3.11 0.13 388 1.32 0.01 1.14 2.40 0.10 340 2.05 0.02 1136.01 1030.42 99.77 360 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.97 0.02 6.75 4.64 0.51 141 2.05 0.02 1323.81 1217.16 99.49 360 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 2.08 0.05 2670898.75 733903.81 100.00 360LCMS-02 8/18/2017 13:08:34 ZLJ_587
Page 1 of 2
MS Report from Instrument: LCMS-02
Ret. Time: 2.08 <<<< POSITIVE SPECTRA >>>> ES-API Positive120000100000800006000040000 362.1200000200300400500600700800900m/z 382.1 742.2 360.1LCMS-02 8/18/2017 13:08:34 ZLJ_587
Page 2 of 2