Data File D:\\AGLIENT...0\\DATA\\20150508-1\\20150508-1 2015-05-08 15-51-47\\BIZ2015-508-DJL6.DSample Name: BIZ2015-508-DJL6=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 18Acq. Instrument : HY-LCMS-02 Location : P2-F-05Injection Date : 5/8/2015 5:07:05 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150508-1\\20150508-1 2015-05-08 15-51-47\\100-1000MS+ 3MIN-1.5_(0.02%FA).MLast changed : 5/8/2015 3:51:47 PM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\1.MLast changed : 5/11/2015 11:25:26 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,Positive,MS:100-1000,Column ID:A-RP-85,50℃ Catalog No : HY-15761 Batch#15985 A-RP-132 Additional Info : Peak(s) manually integrated DAD1 B, Sig=214,4 Ref=off (D:\\AGLIENT...ATA\\20150508-1\\20150508-1 2015-05-08 15-51-47\\BIZ2015-508-DJL6.D) 1.510mAU80060040020000.511.5 1.696 2.131 2.187 2.265 1.995 2.381 2.472 2.754 3.00522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.510 MF 0.0540 2934.38843 906.47467 98.1789 2 1.696 FM 0.0471 9.27974 3.28170 0.3105 3 1.995 MM 0.0532 3.90139 1.22196 0.1305 4 2.131 MF 0.0526 4.80836 1.52265 0.1609 5 2.187 FM 0.0370 5.03353 2.27015 0.1684 6 2.265 MM 0.0390 8.85189e-1 3.78609e-1 0.0296 7 2.381 MM 0.0492 12.40214 4.19741 0.4150 8 2.472 MM 0.0376 2.88800 1.27955 0.0966 9 2.754 MM 0.0525 2.58423 8.20437e-1 0.0865 10 3.005 MM 0.1242 12.64748 1.69761 0.4232 Totals : 2988.81849 923.14475 ===================================================================== *** End of Report ***HY-LCMS-02 5/11/2015 11:25:28 AM Li Shan(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT...0\\DATA\\20150508-1\\20150508-1 2015-05-08 15-51-47\\BIZ2015-508-DJL6.DSample Name: BIZ2015-508-DJL6============================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 18Acq. Instrument : HY-LCMS-02 Location : P2-F-05Injection Date : 5/8/2015 5:07:05 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150508-1\\20150508-1 2015-05-08 15-51-47\\100-1000MS+ 3MIN-1.5_(0.02%FA).MLast changed : 5/8/2015 3:51:47 PM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\1.MLast changed : 5/11/2015 11:26:49 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,Positive,MS:100-1000,Column ID:A-RP-85,50℃ Catalog No : HY-15761 Batch#15985 A-RP-132 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150508-1\\20150508-1 2015-05-08 15-51-47\\BIZ2015-508-DJL6.D) ES-API, Pos, 1.50280000070000060000050000040000030000020000010000000.511.522.53min HY-LCMS-02 5/11/2015 11:26:51 AM Li Shan(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT...0\\DATA\\20150508-1\\20150508-1 2015-05-08 15-51-47\\BIZ2015-508-DJL6.DSample Name: BIZ2015-508-DJL6MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.502 4576515 454.15 I 227.60 I*MSD1 SPC, time=1.471:1.525 of D:\\AGLIENT 1260\\DATA\\20150508-1\\20150508-1 2015-05-08 15-51-47\\BIZ2015-508-DJL6.D ES-100806040200100200300400500600700800900m/z 227.6Max: 511360 *** End of Report ***HY-LCMS-02 5/11/2015 11:26:51 AM Li Shan(LCMS-02) 455.1 454.1Page 2 of 2
