MS Report from Instrument: HY-LCMS-02 File ..M32\\1\\DATA\\20161117\\CPK\\CPK2016-N16-11444.D Tgt Mass (EZX): 424.00 Injection Date : 17 Nov 16 5:53 pm +0800 Seq. Line : 0 Sample Name : CPK2016-N16-11444 Location : P1-B-02 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-10922 Batch#11444 Easy-Access Method: '1-POS-3MIN' 424.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C *DAD1 B, Sig=214,4 Ref=off mAU10001.06350000.5*DAD1 C, Sig=2,4 Ref=off mAU40030020010000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.2451.2491.2991.31.8661.96211.2491.522.5min*1.3121.3501.8671.9471.9791.6161.7801.522.5min*20000010000000.511.5 Ion 425, MSD1 425,Target Mass 424 +H Positive, EIC=424.7:425.7 8000060000400002000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.51.24922.5min22.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.06 0.01 2.17 2.42 0.16 263 1.25 0.02 1350.48 1300.31 97.08 213 1.30 0.02 25.26 6.80 1.82 425 1.36 0.02 2.21 2.28 0.16 425 1.87 0.02 6.12 5.36 0.44 233 1.96 0.02 4.80 4.34 0.35 233 Integration Results for DAD1 C, Sig=2,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.25 0.02 527.58 506.84 93.35 213 1.31 0.03 18.12 11.62 3.21 425 1.35 0.02 3.63 2.79 0. 425 1.62 0.02 3.42 0.24 0.60 233 1.78 0.02 3.22 -0.07 0.57 233 1.87 0.02 3.53 3.12 0.63 233 1.95 0.02 3.41 0.40 0.60 233 1.98 0.02 2.25 1.11 0.40 233HY-LCMS-02 11/18/2016 08:37:01 KFF(LCMS-02)Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 1.25 <<<< POSITIVE SPECTRA >>>> ES-API Positive300002500020000150001000050000200300400500600700800900m/z 426.3 213.2HY-LCMS-02 11/18/2016 08:37:01 KFF(LCMS-02)
425.3Page 2 of 2
